吡啶-1-鎓-4-醇硝酸盐合成路线 （共 5 条）
反应条件
sulfuric acid; nitric acid 1 h; Heating;
参考文献
Houston; Dolence; Keller; Patel-Thombre; Borchardt
Journal of Medicinal Chemistry, 1985 , vol. 28, # 4 p. 467 - 471
反应条件
1: 45 percent / fuming nitric acid, 20percent oleum / 1 h / Heating 2: 94 percent / POCl3, PCl5 / 3 h / Heating View Scheme
参考文献
Houston; Dolence; Keller; Patel-Thombre; Borchardt
Journal of Medicinal Chemistry, 1985 , vol. 28, # 4 p. 467 - 471
反应条件
nitric acid in water
参考文献
Merck and Co., Inc.
Patent: US4038396 A1, 1977 ;
反应条件
1: 45 percent / fuming nitric acid, 20percent oleum / 1 h / Heating 2: 94 percent / POCl3, PCl5 / 3 h / Heating 3: 60.4 percent View Scheme
参考文献
Houston; Dolence; Keller; Patel-Thombre; Borchardt
Journal of Medicinal Chemistry, 1985 , vol. 28, # 4 p. 467 - 471
反应条件
1: 45 percent / fuming nitric acid, 20percent oleum / 1 h / Heating
2: 94 percent / POCl3, PCl5 / 3 h / Heating
3: 60.4 percent
4: 73.4 percent / 0.03 h / 120 °C
View Scheme
参考文献
Houston; Dolence; Keller; Patel-Thombre; Borchardt
Journal of Medicinal Chemistry, 1985 , vol. 28, # 4 p. 467 - 471
