反-二苯乙烯-4,4'-二甲酸二甲酯合成路线 （共 11 条）
反应条件
bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran 2 h; Inert atmosphereReflux;
参考文献
Dieguez, Horacio R.; Lopez, Armando; Domingo, Victoriano; Arteaga, Jesus F.; Dobado, Jose A.; Herrador, M. Mar; Quilez Del Moral, Jose F.; Barrero, Alejandro F.
Journal of the American Chemical Society, 2010 , vol. 132, # 1 p. 254 - 259
反应条件
sodium methylate in tetrahydrofuran T=0°C; Horner-Wadsworth-Emmons olefination; Inert atmosphere;
参考文献
Tovar, John D.
Synthesis, 2011 , # 15 p. 2387 - 2391
反应条件
sulfur T=280°C; P=10343 Torr; 3.33333 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 10 p. 3263 - 3267
反应条件
sulfur in diphenylether T=280°C; P=5171.5 Torr; 8.33333 h; dependence from conc., reaction temp. and time, pressure, solvent; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 56, # 10 p. 3263 - 3267
反应条件
hydrogenchloride; nitrobenzene Erhitzen des Reaktionsprodukts mit Wasser;
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1982
反应条件
1: N-bromosuccinmide; dibenzoyl peroxide / 1,2-dichloro-ethane / Inert atmosphere; Reflux 2: 4-methylmorpholine N-oxide / acetonitrile / 0 °C / Inert atmosphere; Molecular sieve 3: sodium methylate / tetrahydrofuran / 0 °C / Inert atmosphere View Scheme
参考文献
Synthesis, , # 15 p. 2387 - 2391
反应条件
1: 4-methylmorpholine N-oxide / acetonitrile / 0 °C / Inert atmosphere; Molecular sieve 2: sodium methylate / tetrahydrofuran / 0 °C / Inert atmosphere View Scheme
参考文献
Synthesis, , # 15 p. 2387 - 2391
反应条件
methanol; diethyl ether
参考文献
British Journal of Pharmacology and Chemotherapy, , vol. 3, p. 75,76
反应条件
iodine; oxygen in benzene 120 h; Irradiation;
参考文献
Rosa, Joaquin Campos; Galanakis, Dimitrios; Ganellin, C. Robin; Dunn, Philip M.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 21 p. 4247 - 4254
反应条件
sodium hydroxide; ethylene glycol
参考文献
Hager; VanArendonk; Shonle
Journal of the American Chemical Society, 1944 , vol. 66, p. 1982
