甲基7-(5-氧代-1-环戊烯-1-基)庚酸酯合成路线 （共 105 条）
反应条件
sodium methylate; sodium in methanol; water
参考文献
Istituto Biochimico Italiano Giovanni Lorenzini S.p.A.
Patent: US4894473 A1, 1990 ;
反应条件
copper(ll) bromide in chloroform; ethyl acetate
0.666667 h; Heating;
参考文献
Miller, Duane D.; Moorthy, Krishna B.; Hamada, Akihiko
Tetrahedron Letters, 1983 , vol. 24, # 6 p. 555 - 556
反应条件
silver(I) acetate; acetic acid; zinc in methanol
T=60°C; 24 h;
参考文献
Naora, Hirokazu; Ohnuki, Takashi; Nakamura, Asao
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 7 p. 2401 - 2404
反应条件
pyridine; lithium carbonate; N-bromoacetamide in tetrahydrofuran; methanol; water
参考文献
Syntex (U.S.A.) Inc.
Patent: US4046801 A1, 1977 ;
反应条件
p-toluenesulfonic acid monohydrate in methanol
参考文献
American Cyanamid Company
Patent: US4237316 A1, 1980 ;
反应条件
1: 1.) zinc-graphite / 1.) THF, -15 deg C, 30 min, 2.) THF, -78 deg C, 4 h
2: Na2HPO4 / dioxane; H2O / 14 h / Heating
3: PCC, CH3COONa / CH2Cl2 / 2 h / Ambient temperature
4: 78 percent / CH3ONa / methanol
View Scheme
参考文献
Boga, Carla; Savoia, Diego; Trombini, Claudio; Umani-Ronchi, Achille
Journal of Chemical Research, Miniprint, 1985 , # 7 p. 2461 - 2472
参考文献
Sih; Salomon; Price; Sood; Peruzzotti
Journal of the American Chemical Society, 1975 , vol. 97, # 4 p. 857 - 865
反应条件
toluene-4-sulfonic acid
5 h; Heating;
参考文献
Bernady; Poletto; Nocera; et al.
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4702 - 4715
反应条件
manganese(IV) oxide in Petroleum ether
24 h; Ambient temperature;
参考文献
Novak; Baan; Marosfalvi; Szantay
Chemische Berichte, 1980 , vol. 113, # 9 p. 2939 - 2949
反应条件
hydrogenchloride in methanol
8 h; Heating;
参考文献
Ono, Noboru; Miyake, Hideyoshi; Kaji, Aritsume
Synthesis, 1981 , # 12 p. 1003 - 1004
