4,4'-二甲基苯偶酰合成路线 （共 111 条）
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-(+)-1,1'-binaphthyl-2,2'-diamine in toluene T=60°C; 10 h; optical yield given as percent eeenantioselective reaction;
参考文献
Alamsetti, Santosh Kumar; Mannam, Sreedevi; Mutupandi, Pandi; Sekar, Govindasamy
Chemistry - A European Journal, 2009 , vol. 15, # 5 p. 1086 - 1090
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-(+)-1,1'-binaphthyl-2,2'-diamine in toluene T=60°C; 12 h; optical yield given as percent eeenantioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 15, # 5 p. 1086 - 1090
反应条件
copper(I) bromide; lithium bromide in tetrahydrofuran T=0°C; 0.25 h;
参考文献
Babudri, Francesco; Fiandanese, Vito; Marchese, Giuseppe; Punzi, Angela
Tetrahedron Letters, 1995 , vol. 36, # 40 p. 7305 - 7308
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Wang, Xiaoxia; Zhang, Yongmin
Tetrahedron Letters, 2002 , vol. 43, # 31 p. 5431 - 5433
反应条件
1: With tetra-n-butylammonium tetrafluoroborate; dimethyl sulfoxide in dichloromethane T=0°C; ElectrolysisInert atmosphere; 2: With triethylamine in dichloromethane T=35°C; 1 h; Inert atmosphere;
参考文献
Ashikari, Yosuke; Nokami, Toshiki; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2011 , vol. 133, # 31 p. 11840 - 11843
反应条件
lithium in tetrahydrofuran 54 h; Ambient temperatureultrasonic bath;
参考文献
Karaman; Fry
Tetrahedron Letters, 1989 , vol. 30, # 46 p. 6267 - 6270
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine T=145°C; 15 h; Yields of byproduct given;
参考文献
Rich, Jonathan D.
Journal of the American Chemical Society, 1989 , vol. 111, # 15 p. 5886 - 5893
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Wang, Xiaoxia; Zhang, Yongmin
Tetrahedron, 2003 , vol. 59, # 23 p. 4201 - 4207
反应条件
selenium(IV) oxide in dimethyl sulfoxide 0.0111111 h; microwave irradiation;
参考文献
Ramajayam; Giridhar, Rajani; Yadav; Balaraman; Djaballah, Hakim; Shum, David; Radu, Constantin
European Journal of Medicinal Chemistry, 2008 , vol. 43, # 9 p. 2004 - 2010
反应条件
in tetrahydrofuran T=65°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 33, # 15 p. 1941 - 1944
