4,4'-二甲基苯偶酰合成路线 （共 111 条）
反应条件
1: 74 percent / bis(trifluoroacetoxy)iodobenzene, water / CHCl3 / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 10 p. 1967 - 1969
Zhurnal Organicheskoi Khimii, , vol. 23, # 10 p. 2225 - 2227
反应条件
1.1: Mg / tetrahydrofuran 1.2: dichloro[1,3-bis(diphenylphosphino)ethane]nickel(II) / tetrahydrofuran 2.1: SeO2; 90 percent aq. AcOH; H2SO4 View Scheme
参考文献
Journal of Materials Chemistry, , vol. 11, # 4 p. 1063 - 1071
反应条件
1: Na(1+)*(SiMe3)2N(1-) / tetrahydrofuran / -60 °C 2: tetrahydrofuran / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 119, # 4 p. 1350 - 1360
反应条件
1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 3 h / 0 °C / |Inert atmosphere 1.2: 4 h / 20 °C / |Inert atmosphere 2.1: hydrogen / methanol / 5 h / 3620.13 Torr / |Inert atmosphere 3.1: pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 39 p. 5327 - 5330
反应条件
aluminium trichloride T=40°C; 1 h; Further byproducts given;
参考文献
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, , vol. 276-277, # pt 1-2 p. 271 - 275
反应条件
sodium hydroxide; selenium(IV) oxide 1.) DMF, 78-80 deg C; 2.) THF, r.t.; Yield given. Multistep reaction;
参考文献
Synlett, , vol. 1997, # 6 p. 671 - 672
反应条件
hydrogenchloride 14 h;
参考文献
Chemistry Letters, , vol. 33, # 2 p. 102 - 103
反应条件
dodecacarbonyltriiron in benzene T=80°C; 20 h; Heatingdifferent reaction times; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 1 p. 118 - 122
反应条件
oxygen; pyridine; compound with copper (II)-nitrate in methanol T=25°C; 9 h; competitive reaction; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3498 - 3503
反应条件
hydrogenchloride; water 1.) THF, 0 deg C, 2 h; 2.) THF, reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 521, # 1-2 p. 121 - 124
