反应条件
carbon monoxide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane
High Pressure; 1.76 mmol PhCOCl, 2 ml of Et3Al in hexane (1 M), 3 ml THF, 0.05 mmol Pd complex, CO 70 atm, stirred for 46 h at 25°C, mixture dissolved in 70percent AcOH (3 ml), 1 mmol Cu(OAc)2 added, stirred for about 1 h at 100°C; GC-MS, GC;
参考文献
Yamashita, Hiroshi; Kobayashi, Toshi-aki; Sakakura, Toshiyasu; Tanaka, Masato
Journal of Organometallic Chemistry, 1988 , vol. 356, p. 125 - 132
