3-(苯基甲基)戊烷-3-醇合成路线 （共 29 条）
反应条件
copolymer of 2-vinylnaphth. + divinylbenzene; lithium in tetrahydrofuran T=-78 - 20°C;
参考文献
Candela; Gomez; Yus
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 6 p. 795 - 801
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=-78 - 20°C; 4 h;
参考文献
Guijarro; Yus
Tetrahedron, 1994 , vol. 50, # 11 p. 3447 - 3452
反应条件
naphthalene; lithium in tetrahydrofuran T=-30°C; Barbier-type reaction; 3 h;
参考文献
Guijarro, David; Yus, Miguel
Journal of Organometallic Chemistry, 2001 , vol. 624, # 1-2 p. 53 - 57
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0°C; 2 h;
参考文献
Yus, Miguel; Martinez, Pedro; Guijarro, David
Synthetic Communications, 2003 , vol. 33, # 13 p. 2365 - 2376
反应条件
naphthalene; lithium in tetrahydrofuran T=-78°C; Condensation; 5 h;
参考文献
Alonso, Emma; Guijarro, David; Martinez, Pedro; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1999 , vol. 55, # 36 p. 11027 - 11038
反应条件
1: phenylmethanethiol With n-butyllithium in tetrahydrofuran; hexane T=20°C; 0.0833333 h; 2: With 4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran; hexane T=0°C; 1 h; 3: pentan-3-one in tetrahydrofuran; hexane T=-30 - 0°C; 3 h;
参考文献
Yus, Miguel; Martinez, Pedro; Guijarro, David
Synthetic Communications, 2003 , vol. 33, # 13 p. 2365 - 2376
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0°C; 2 h;
参考文献
Yus, Miguel; Martinez, Pedro; Guijarro, David
Synthetic Communications, 2003 , vol. 33, # 13 p. 2365 - 2376
反应条件
Ph(Me)Cu(CN)Li2 in tetrahydrofuran T=0°C; 3.5 h; Yield given. Yields of byproduct given;
参考文献
Lipshutz, Bruce H.; Wilhelm, Robert S.; Kozlowski, Joseph A.; Parker, David
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3928 - 3938
反应条件
1: dibenzyl disulphide With 4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0°C; 1 h; 2: pentan-3-one in tetrahydrofuran T=-30 - 0°C; 3 h;
参考文献
Yus, Miguel; Martinez, Pedro; Guijarro, David
Synthetic Communications, 2003 , vol. 33, # 13 p. 2365 - 2376
反应条件
1: 50 percent / 4-(N,N-dimethylamino)pyridine 2: 50 percent / Li; naphthalene / tetrahydrofuran / 2 h / -30 °C View Scheme
参考文献
Alonso, Emma; Guijarro, David; Yus, Miguel
Tetrahedron, 1995 , vol. 51, # 42 p. 11457 - 11464
