9,10-二溴-9,10-二氢-4H-苯并[4,5]环庚并[1,2-b]噻吩-4-酮合成路线 （共 4 条）
反应条件
N-bromosuccinmide; dibenzyl peroxide in tetrachloromethane 3 h; Heating;
参考文献
Polivka, Zdenek; Budesinsky, Milos; Holubek, Jiri; Schneider, Bohdan; Sediva, Zdenek; et al.
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 9 p. 2443 - 2469
反应条件
mother liquors after XXIV diluted warwe and extracted with dichlormethane; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Polivka, Zdenek; Budesinsky, Milos; Holubek, Jiri; Schneider, Bohdan; Sediva, Zdenek; et al.
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 9 p. 2443 - 2469
反应条件
1: mother liquors after XXIV diluted warwe and extracted with dichlormethane 2: Mg / 1)Grignard reagent in THF 2)15 deg C, 50min, educt XXIV 3)1.5h room temp. View Scheme
参考文献
Polivka, Zdenek; Budesinsky, Milos; Holubek, Jiri; Schneider, Bohdan; Sediva, Zdenek; et al.
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 9 p. 2443 - 2469
反应条件
1: mother liquors after XXIV diluted warwe and extracted with dichlormethane 2: Mg / 1)Grignard reagent in THF 2)15 deg C, 50min, educt XXIV 3)1.5h room temp. 3: 97 percent / HCl / H2O / 1 h / Heating View Scheme
参考文献
Polivka, Zdenek; Budesinsky, Milos; Holubek, Jiri; Schneider, Bohdan; Sediva, Zdenek; et al.
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 9 p. 2443 - 2469
