5-溴-2-甲基-3-呋喃羧酸甲酯合成路线 (共 4 条)
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide T=0 - 50°C; 1 h;
参考文献
Tang, Bencan; Bray, Christopher D.; Pattenden, Gerald; Rogers, Joseph
Tetrahedron, 2010 , vol. 66, # 13 p. 2492 - 2500
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 14 h; Heating;
参考文献
Khatuya, Haripada
Tetrahedron Letters, 2001 , vol. 42, # 14 p. 2643 - 2644
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 20 h; Heating; Product distribution; Further Variations:Reaction partnersReagentsSolventsTemperaturesreaction times;
参考文献
Khatuya, Haripada
Tetrahedron Letters, 2001 , vol. 42, # 14 p. 2643 - 2644
反应条件
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether; water / 16 h / 85 °C 2: water; lithium hydroxide hydrate / methanol / Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 18 p. 5417 - 5422