4-硝基苯基-2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖苷合成路线 （共 37 条）
反应条件
Thermus nonproteolyticus HG102 E338A mutant; glycine; sodium hydroxide in N,N-dimethyl-formamide T=45°C; pH=8.8; 48 h; Enzymatic reaction;
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
Bacillus circulans β-galactosidase in phosphate buffer; acetonitrile T=30°C; pH=6.8; 24 h;
参考文献
Carbohydrate Research, , vol. 340, # 16 p. 2469 - 2475
反应条件
1.1: 95 percent / pyridine / 16 h / 20 °C 2.1: CH2Cl2 / 2 h / 20 °C 2.2: BF3*OEt2 / CH2Cl2 / -30 °C 2.3: 53 percent / pyridine / 20 - 48 °C 3.1: 85 percent / HF-pyridine / 48 h 4.1: 78 percent / NaOMe / methanol / 2 h / 20 °C View Scheme
参考文献
Clinch, Keith; Evans, Gary B; Furneaux, Richard H; Rendle, Phillip M; Rhodes, Phillippa L; Roberton, Anthony M; Rosendale, Douglas I; Tyler, Peter C; Wright, Damian P
Carbohydrate Research, 2002 , vol. 337, # 12 p. 1095 - 1111
反应条件
in acetonitrile T=30°C; 8 h; β-D-galactosidase from Bacillus circulans, phosphate buffer;
参考文献
Carbohydrate Research, , vol. 244, # 2 p. 315 - 323
反应条件
β4galT; manganese (II) chloride; bovine serum albumin in various solvent(s) T=37°C; pH=7.5; Enzymatic reaction; Product distribution; Further Variations:Reagents;
参考文献
Blixt; Brown; Schur; Wakarchuk; Paulson
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2442 - 2448
反应条件
β-galactosidase in acetonitrile Enzymatic reaction;
参考文献
Kanno, Kenichi; Kawazumi, Hirofumi; Miyazaki, Masaya; Maeda, Hideaki; Fujii, Masayuki
Australian Journal of Chemistry, 2002 , vol. 55, # 11 p. 687 - 690
反应条件
Uridine diphosphate galactose; dimyristoyl-phosphatidylcholine; manganese (II) chloride in water T=37°C; pH=7; aq. bufferEnzymatic reaction; Kinetics; Concentration;
参考文献
Noble, Gavin T.; Craven, Faye L.; Voglmeir, Josef; Sardzik, Robert; Flitsch, Sabine L.; Webb, Simon J.
Journal of the American Chemical Society, 2012 , vol. 134, # 31 p. 13010 - 13017
反应条件
1: 4-TsOH*H2O / dimethylformamide / 20 °C 2: pyridine / 1.5 h / 0 °C 3: 6.19 g / AcOH; H2O / 3 h / 70 °C 4: 86 percent / pyridine / CH2Cl2 / 20 °C View Scheme
参考文献
Chen, Hong-Ming; Withers, Stephen G.
Carbohydrate Research, 2007 , vol. 342, # 15 p. 2212 - 2222
反应条件
T=37°C; 80 h; glycosidase precipitate (from livers of the mollusc Chamelea gallina), 0.03M sodium citrate/phosphate buffer pH 5.8; Yields of byproduct given;
参考文献
Nilsson
Carbohydrate research, 1990 , vol. 204, p. 79 - 83
反应条件
1.1: pyridine 1.2: pyridine 2.1: KCN / dimethylformamide / 90 °C View Scheme
参考文献
Carmona, Ana T.; Fialova, Pavla; Kren, Vladimir; Ettrich, Rudiger; Martinkova, Ludmila; Moreno-Vargas, Antonio J.; Gonzalez, Cristina; Robina, Inmaculada
European Journal of Organic Chemistry, 2006 , # 8 p. 1876 - 1885
