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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3459-94-7
合成路线
（共 33 条）
624-38-4
1,4-二碘苯
+
108-98-5
硫酚
→
反应条件
3459-94-7
反应条件
tetra(n-butyl)ammonium hydroxide in water T=50°C; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Xu, Hua-Jian; Liang, Yu-Feng; Zhou, Xin-Feng; Feng, Yi-Si
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2562 - 2568
637-87-6
对氯碘苯
+
108-98-5
硫酚
→
反应条件
3459-94-7
反应条件
1.2.3.4-tetrahydro-8-hydroxy-quinoline; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=130°C; 48 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yaming; Li, Xiaoying; Wang, Huifeng; Chen, Tao; Xie, Yusheng
Synthesis, 2010 , # 21 art. no. F10410SS, p. 3602 - 3608
589-87-7
对溴碘苯
+
108-98-5
硫酚
→
反应条件
3459-94-7
反应条件
1.2.3.4-tetrahydro-8-hydroxy-quinoline; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=130°C; 48 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yaming; Li, Xiaoying; Wang, Huifeng; Chen, Tao; Xie, Yusheng
Synthesis, 2010 , # 21 art. no. F10410SS, p. 3602 - 3608
106-37-6
对二溴苯
+
108-98-5
硫酚
→
反应条件
3459-94-7
反应条件
1.2.3.4-tetrahydro-8-hydroxy-quinoline; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=130°C; 48 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yaming; Li, Xiaoying; Wang, Huifeng; Chen, Tao; Xie, Yusheng
Synthesis, 2010 , # 21 art. no. F10410SS, p. 3602 - 3608
106-46-7
对二氯苯
+
108-98-5
硫酚
→
反应条件
3459-94-7
反应条件
1.2.3.4-tetrahydro-8-hydroxy-quinoline; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=130°C; 48 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yaming; Li, Xiaoying; Wang, Huifeng; Chen, Tao; Xie, Yusheng
Synthesis, 2010 , # 21 art. no. F10410SS, p. 3602 - 3608
589-87-7
对溴碘苯
+
882-33-7
二苯二硫醚
→
反应条件
3459-94-7
反应条件
copper(I) oxide; [2,2']bipyridinyl; magnesium in N,N-dimethyl-formamide T=110°C; 72 h;
参考文献
Taniguchi, Nobukazu; Onami, Tetsuo
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 915 - 920
106-39-8
4-溴氯苯
+
108-98-5
硫酚
→
反应条件
3459-94-7
反应条件
1.2.3.4-tetrahydro-8-hydroxy-quinoline; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=130°C; 48 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yaming; Li, Xiaoying; Wang, Huifeng; Chen, Tao; Xie, Yusheng
Synthesis, 2010 , # 21 art. no. F10410SS, p. 3602 - 3608
52599-10-7
→
反应条件
623-26-7
对苯二腈
+
3459-94-7
+
65662-88-6
4-溴二苯硫醚
+
51238-46-1
反应条件
n-Bu4N+CN- in dimethyl sulfoxide T=25°C; 1 h; Irradiation;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Dell'erba, Carlo
Tetrahedron, 1987 , vol. 43, # 20 p. 4625 - 4634
52599-10-7
+
10442-39-4
氰化四丁基铵
→
反应条件
623-26-7
对苯二腈
+
3459-94-7
+
65662-88-6
4-溴二苯硫醚
+
51238-46-1
反应条件
n-Bu4N+CN- in dimethyl sulfoxide T=25°C; 1 h; Irradiation;
参考文献
Tetrahedron, , vol. 43, # 20 p. 4625 - 4634
673-41-6
+
930-69-8
苯硫酚钠
→
反应条件
3459-94-7
+
13343-26-5
4-氯二苯硫醚
反应条件
in dimethyl sulfoxide T=25°C; 3 h;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Dell'Erba, Carlo
Tetrahedron, 1986 , vol. 42, # 14 p. 4007 - 4016
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