(4-乙炔基苯基)(4-吡啶基)甲酮合成路线 （共 5 条）
反应条件
1.1: SOCl2 2.1: CuI; Pd(PPh3)2Cl2; diisopropylamine / benzene / 20 °C 2.2: NaOH / methanol / 12 h / 20 °C View Scheme
参考文献
Leventis, Nicholas; Elder, Ian A.; Gao, Xuerong; Bohannan, Eric W.; Sotiriou-Leventis, Chariklia; Rawashdeh, Abdel Monem M.; Overschmidt, Travis J.; Gaston, Kimberly R.
Journal of Physical Chemistry B, 2001 , vol. 105, # 17 p. 3663 - 3674
反应条件
sodium hydroxide in methanol T=23°C; 14 h;
参考文献
Leventis, Nicholas; Elder, Ian A.; Gao, Xuerong; Bohannan, Eric W.; Sotiriou-Leventis, Chariklia; Rawashdeh, Abdel Monem M.; Overschmidt, Travis J.; Gaston, Kimberly R.
Journal of Physical Chemistry B, 2001 , vol. 105, # 17 p. 3663 - 3674
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine in benzene T=20°C; 2: With sodium hydroxide in methanol T=20°C; 12 h; Further stages.;
参考文献
Leventis, Nicholas; Rawaswdeh, Abdel-Monem M.; Zhang, Guohui; Elder, Ian A.; Sotiriou-Leventis, Chariklia
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7501 - 7510
反应条件
1: 28.4 g / AlCl3 / 0 - 90 °C 2: i-Pr2NH / Pd(PPh3)2Cl2; CuI / benzene / 14 h / 23 °C 3: 1.91 g / NaOH / methanol / 14 h / 23 °C View Scheme
参考文献
Leventis, Nicholas; Rawaswdeh, Abdel-Monem M.; Zhang, Guohui; Elder, Ian A.; Sotiriou-Leventis, Chariklia
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7501 - 7510
反应条件
1: i-Pr2NH / Pd(PPh3)2Cl2; CuI / benzene / 14 h / 23 °C 2: 1.91 g / NaOH / methanol / 14 h / 23 °C View Scheme
参考文献
Leventis, Nicholas; Elder, Ian A.; Gao, Xuerong; Bohannan, Eric W.; Sotiriou-Leventis, Chariklia; Rawashdeh, Abdel Monem M.; Overschmidt, Travis J.; Gaston, Kimberly R.
Journal of Physical Chemistry B, 2001 , vol. 105, # 17 p. 3663 - 3674
