反应条件
1.1: 97 percent / pyridine / ethanol
2.1: n-BuLi / tetrahydrofuran / -60 °C
2.2: 65 percent / tetrahydrofuran / -60 °C
3.1: LDA / tetrahydrofuran / -60 °C
3.2: tetrahydrofuran / -60 °C
4.1: TBAF / tetrahydrofuran
5.1: 94 percent / oxalyl chloride; DMSO; triethylamine / CH2Cl2 / -60 - 20 °C
View Scheme
参考文献
Takle, Andrew K.; Brown, Murray J.B.; Davies, Susannah; Dean, David K.; Francis, Gerraint; Gaiba, Alessandra; Hird, Alex W.; King, Frank D.; Lovell, Peter J.; Naylor, Antoinette; Reith, Alastair D.; Steadman, Jon G.; Wilson, David M.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 2 p. 378 - 381
