反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / N,N-dimethyl-formamide / 1 h / 0 - 20 °C
2: tri-isopropoxy-borane; lithium diisopropyl amide / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
View Scheme
参考文献
Herdemann, Matthias; Weber, Alexander; Jonveaux, Jerome; Schwoebel, Frank; Stoeck, Michael; Heit, Isabelle
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 6 p. 1852 - 1856