3-(苄氧羰基氨基)-1-丙醇合成路线 （共 22 条）
反应条件
sodium hydroxide T=0 - 25°C; Substitution; 4 h;
参考文献
Geall, Andrew J.; Blagbrough, Ian S.
Tetrahedron, 2000 , vol. 56, # 16 p. 2449 - 2460
反应条件
anhydrous sodium hydrogen carbonate in 1,4-dioxane; water; ethyl acetate
参考文献
Meiji Seika Kaisha, Ltd.; Bayer Aktiengesellschaft
Patent: US6329338 B1, 2001 ;
反应条件
sodium tetrahydroborate in tetrahydrofuran T=0°C; Reduction; 5 h;
参考文献
Journal of the American Chemical Society, , vol. 121, # 49 p. 11356 - 11368
反应条件
in dichloromethane T=20°C; 0.0833333 h;
参考文献
Shimizu, Mamoru; Sodeoka, Mikiko
Organic Letters, 2007 , vol. 9, # 25 p. 5231 - 5234
反应条件
triethylamine in methanol; ethyl acetate 0.5 h;
参考文献
Gening; Tsvetkov; Pier; Nifantiev
Russian Journal of Bioorganic Chemistry, 2006 , vol. 32, # 4 p. 389 - 399
反应条件
triethylamine in 1,4-dioxane; water 2 h; Ambient temperature;
参考文献
Fushiya, Shinji; Kanazawa, Toshiyuki; Nozoe, Shigeo
Bioorganic and Medicinal Chemistry, 1997 , vol. 5, # 11 p. 2089 - 2094
反应条件
triethylamine in methanol 1 h; Heating;
参考文献
DeMong, Duane E.; Williams, Robert M.
Tetrahedron Letters, 2001 , vol. 42, # 2 p. 183 - 185
反应条件
1: Et3N / tetrahydrofuran / 2 h / 0 °C 2: aq. sodium borohydride / tetrahydrofuran / 5 h / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 121, # 49 p. 11356 - 11368
反应条件
1: aq. NaHCO3 / dioxane / 3.75 h / 0 - 20 °C 2: Et3N / tetrahydrofuran / 2 h / 0 °C 3: aq. sodium borohydride / tetrahydrofuran / 5 h / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 121, # 49 p. 11356 - 11368
反应条件
triethylamine in dichloromethane T=25°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 18, # 10 p. 3518 - 3534
