3,3A,6,6A-四氢-2H-环戊二烯并[b]呋喃-2-酮合成路线 （共 47 条）
反应条件
oxygen in water T=30°C; 2 h; biotransformation by Ps. putida NCIMB 10007 monooxygenase enzyme using NADPH as cofactor; further monooxygenases; pH 7.1; Yield given. Yields of byproduct given;
参考文献
Cavarzan, Alessandra; Bianchini, Giulio; Sgarbossa, Paolo; Lefort, Laurent; Gladiali, Serafino; Scarso, Alessandro; Strukul, Giorgio
Chemistry - A European Journal, 2009 , vol. 15, # 32 p. 7930 - 7939
反应条件
dihydrogen peroxide; acetic acid T=0°C; 12 h;
参考文献
Corey; Su, Wei-Guo
Tetrahedron Letters, 1990 , vol. 31, # 27 p. 3833 - 3836
反应条件
oxygen in water T=30°C; 1 h; biotransformation by Ps. putida NCIMB 10007 monooxygenase enzyme using NADH as cofactor; further monooxygenases; pH 7.1; Yield given. Title compound not separated from byproducts;
参考文献
Gadnon, Rene; Grogan, Gideon; Levitt, Melissa S.; Roberts, Stanley M.; Wan, Peter W. H.; Willetts, Andrew J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 18 p. 2537 - 2544
反应条件
sodium hydroxide in tetrahydrofuran; water
参考文献
Hoffmann-La Roche Inc.
Patent: US3933892 A1, 1976 ;
反应条件
sulfuric acid in pyridine
参考文献
Hoffmann-La Roche Inc.
Patent: US3933892 A1, 1976 ;
反应条件
pyridine in benzene T=240 - 250°C; 0.5 h;
参考文献
Weinges, Klaus; Schwarz, Georg
Liebigs Annalen der Chemie, 1993 , # 7 p. 811 - 814
反应条件
ammonium chloride; zinc in methanol 2 h; Heating;
参考文献
Kitahara, Takeshi; Nishi, Tsunehiro; Mori, Kenji
Tetrahedron, 1991 , vol. 47, # 34 p. 6999 - 7006
反应条件
ethylenediaminetetraacetic acid; oxygen; Adenine-flavine dinucleotide; NADP in water T=30°C; Baeyer-Villiger oxidation reaction; pH=7.4; Irradiationkinetic resolution;
参考文献
Jensen, Chantel N.; Cartwright, Jared; Ward, Jonathan; Hart, Sam; Turkenburg, Johan P.; Ali, Sohail T.; Allen, Michael J.; Grogan, Gideon
ChemBioChem, 2012 , vol. 13, # 6 p. 872 - 878
反应条件
phosphite dehydrogenase; Cyanidioschyzon merolae strain 10D (NIES-1332) Baeyer-Villiger monooxygenase; anhydrous phosphate; NADPH in 1,4-dioxane T=25°C; Baeyer-Villiger Ketone Oxidation; pH=7.5; Enzymatic reaction; Kinetics; Reagent/catalyst; regioselective reaction;
参考文献
Beneventi, Elisa; Niero, Mattia; Motterle, Riccardo; Fraaije, Marco; Bergantino, Elisabetta
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 98, p. 145 - 154
反应条件
chromium(VI) oxide; sulfuric acid in water; acetone 1) 0 deg C, 1h, 2) RT, 2h;
参考文献
Busato, Stephan; Tinembart, Olivier; Zhang, Zhong-da; Scheffold, Rolf
Tetrahedron, 1990 , vol. 46, # 9 p. 3155 - 3166
