diisobutylaluminium hydride in tetrahydrofuran; pentane T=-78°C; 4 h;
参考文献
Broom, Nigel; O'Hanlon, Peter J.; Simpson, Thomas J.; Stephen, Rosamund; Willis, Christine L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 24 p. 3067 - 3072
1: singlet oxygen / 0 °C / temperature must not exceed 0 deg C 2: 83 percent / tetrahydrofuran / 0.5 h / -78 - 0 °C 3: 90 percent / xylene / Heating View Scheme
参考文献
Schwaebe, Michael K.; Little, R. Daniel
Tetrahedron Letters, 1996 , vol. 37, # 37 p. 6635 - 6638
