2-(4-溴苯基)咪唑并[1,2-a]吡啶合成路线 (共 19 条)
反应条件
1: 64 percent / acetone / 12 h / Ambient temperature 2: 96 percent / Et3N / methanol / 4 h / Heating View Scheme
参考文献
Synthesis, , # 8 p. 927 - 929
反应条件
1: tetrahydrofuran / Ambient temperature 2: potassium carbonate / tetrahydrofuran / 72 h View Scheme
参考文献
Heterocycles, , vol. 32, # 12 p. 2373 - 2380
反应条件
1: tetrahydrofuran / Ambient temperature 2: potassium carbonate / tetrahydrofuran / 72 h View Scheme
参考文献
Heterocycles, , vol. 32, # 12 p. 2373 - 2380
反应条件
1: 81 percent / tetrahydrofuran / 0.25 h / 60 °C 2: tetrahydrofuran / Ambient temperature 3: potassium carbonate / tetrahydrofuran / 72 h View Scheme
参考文献
Heterocycles, , vol. 32, # 12 p. 2373 - 2380
反应条件
ammonium acetate T=180°C; 0.0666667 h; Microwave irradiationneat (no solvent);
参考文献
Synlett, , # 11 p. 1606 - 1608
反应条件
1.) acetone, rt, 3 d, 2.) pyridine, heating, 12 h; Yield given. Multistep reaction;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 4 p. 548 - 553
Zhurnal Organicheskoi Khimii, , vol. 31, # 4 p. 595 - 600
反应条件
1: N-iodo-succinimide / acetonitrile / 1 h / 20 °C 2: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 18 h / 80 °C View Scheme
参考文献
Samsung Mobile Display Co., Ltd.
Patent: EP2292601 A1, 2011 ;
反应条件
1: 56 percent / dimethylformamide / 24 h / Heating 2: 60 percent / sodium hypophosphite hydrate / Ra-Ni / H2O; acetic acid; pyridine / 7 h / 100 °C View Scheme
参考文献
Sundberg; Dahlhausen; Manikumar; Mavunkel; Biswas; Srinivasan; King Jr.; Waid
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 1 p. 129 - 137
反应条件
in N,N-dimethyl-formamide
24 h; Heating;
参考文献
Sundberg; Dahlhausen; Manikumar; Mavunkel; Biswas; Srinivasan; King Jr.; Waid
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 1 p. 129 - 137