N-(2,5-二甲氧基苯基)乙酰胺合成路线 （共 14 条）
反应条件
N-ethyl-N,N-diisopropylamine in chloroform 1.5 h;
参考文献
WO2008/76524 A2, ;
Page/Page column 83 ;
反应条件
triethylamine in dichloromethane 1 h; Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 111, # 20 p. 7932 - 7938
反应条件
iodine; triphenylphosphine in acetonitrile Beckmann rearrangement; 0.0833333 h; Reflux;
参考文献
Synthetic Communications, , vol. 42, # 23 p. 3532 - 3539
反应条件
polyphosphoric acid T=105 - 110°C; 3 h;
参考文献
Synlett, , # 17 p. 2628 - 2630
参考文献
Journal of Organic Chemistry, , vol. 60, # 13 p. 4268 - 4271
反应条件
1: sodium amalgam View Scheme
参考文献
Chemische Berichte, , vol. 17, p. 2124
反应条件
1: 91 percent / KOH / dimethylsulfoxide / 0.5 h / Ambient temperature 2: 98 percent / HCl / H2O / 5 h / 100 °C View Scheme
参考文献
Russell, Richard A.; Longmore, Robert W.; Warrener, Ronald N.
Australian Journal of Chemistry, 1991 , vol. 44, # 12 p. 1691 - 1704
反应条件
potassium hydroxide; acetone anschliessendes Hydrolisieren;
参考文献
Loudon; Ogg
Journal of the Chemical Society, 1955 , p. 739,743
反应条件
(i) NaH, xylene, (ii) /BRN= 635994/, (iii) aq. H2SO4; Multistep reaction;
参考文献
Walker; Daisley; Beckett
Journal of medicinal chemistry, 1970 , vol. 13, # 5 p. 983 - 985
反应条件
1: glacial acetic acid; nitric acid / 5 °C 2: alcoholic hydrochloric acid View Scheme
参考文献
Rubenstein
Journal of the Chemical Society, 1925 , vol. 127, p. 2003
