3,5-二甲基苯基溴化镁合成路线 （共 25 条）
反应条件
magnesium in tetrahydrofuran
参考文献
Journal of the American Chemical Society, , vol. 109, # 10 p. 3098 - 3107
反应条件
1: absolute diethyl ether 2: Cr2O3-H2SO4 View Scheme
参考文献
v.Auwers; Lechner; Bundesmann
Chemische Berichte, 1925 , vol. 58, p. 41
反应条件
2: I2 3: H2 / Raney-Ni / ethanol View Scheme
参考文献
Repinskaya,I.B. et al.
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 10 p. 2143 - 2149,2225 - 2230
反应条件
1.1: LDA / tetrahydrofuran / -78 °C 1.2: 56 percent / tetrahydrofuran / -78 °C 2.1: 99 percent / H2O2 / acetone / 0 °C 3.1: Cu / dimethylformamide / 140 °C 3.2: (-)-L-DBTA / resolution of racemate 4.1: HSiCl3; Et3N View Scheme
参考文献
Wu, Jing; Chen, Hua; Kwok, Wai Him; Lam, Kim Hung; Zhou, Zhong Yuan; Yeung, Chi Hung; Chan, Albert S.C
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1539 - 1543
参考文献
Repinskaya,I.B. et al.
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 10 p. 2143 - 2149,2225 - 2230
反应条件
1.1: LDA / tetrahydrofuran / -78 °C 1.2: 56 percent / tetrahydrofuran / -78 °C 2.1: 99 percent / H2O2 / acetone / 0 °C 3.1: Cu / dimethylformamide / 140 °C 3.2: (-)-L-DBTA / resolution of racemate 4.1: HSiCl3; Et3N View Scheme
参考文献
Wu, Jing; Chen, Hua; Kwok, Wai Him; Lam, Kim Hung; Zhou, Zhong Yuan; Yeung, Chi Hung; Chan, Albert S.C
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1539 - 1543
反应条件
tri-isopropoxy-borane in tetrahydrofuran T=-55 - 20°C; Temperature;
参考文献
Winkle, Derick D.; Schaab, Kevin M.
Organic Process Research and Development, 2001 , vol. 5, # 4 p. 450 - 451
反应条件
monobutyl butyl phosphonate; potassium hydride in diethyl ether 4 h;
参考文献
Journal of the American Chemical Society, , vol. 116, # 22 p. 9869 - 9882
参考文献
Schubert et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 5462,5465
参考文献
Castro et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 2322,2324
