3,5-二甲基苯基溴化镁合成路线 （共 25 条）
参考文献
Casalnuovo, Albert L.; RajanBabu, T. V.; Ayers, Timothy A.; Warren, Timothy H.
Journal of the American Chemical Society, 1994 , vol. 116, # 22 p. 9869 - 9882
参考文献
Wu, Jing; Chen, Hua; Kwok, Wai Him; Lam, Kim Hung; Zhou, Zhong Yuan; Yeung, Chi Hung; Chan, Albert S.C
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1539 - 1543
反应条件
phosphorus trichoride in tetrahydrofuran 0 deg C then reflux, 2 h;
参考文献
Culcasi, Marcel; Berchadsky, Yves; Gronchi, Gerard; Tordo, Paul
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3537 - 3542
参考文献
Nauta; Ernsting; Faber
Recueil des Travaux Chimiques des Pays-Bas, 1941 , vol. 60, p. 915,927
参考文献
Murata; Goto; Fujiyama; Mishima; Fujio; Tsuno
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 4 p. 1129 - 1137
参考文献
Mathre, David J.; Jones, Todd K.; Xavier, Lyndon C.; Blacklock, Thomas J.; Reamer, Robert A.; et al.
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 751 - 762
参考文献
Nishida,S.
Journal of Organic Chemistry, 1967 , vol. 32, p. 2695 - 2697
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Grunert; Nichol; Sandin
Journal of the American Chemical Society, 1947 , vol. 69, p. 2254
反应条件
1.1: HCl 2.1: O2 / benzene 3.1: Mg; I2 / tetrahydrofuran; toluene / 75 °C 3.2: 71 percent / tetrahydrofuran; toluene / 16 h / 60 °C 4.1: 96 percent / (EtO)3P; HSiCl3 / tetrahydrofuran; toluene / 2 h / 100 °C View Scheme
参考文献
Wu, Hai-Chen; Yu, Jin-Quan; Spencer, Jonathan B.
Organic Letters, 2004 , vol. 6, # 25 p. 4675 - 4678
参考文献
Baker,P.B. et al.
Tetrahedron, 1973 , vol. 29, p. 85 - 91
反应条件
sulfuric acid; water byproducts: H2O; dehydration with petroleum ether;;
参考文献
Gmelin Handbook: B: B-Verb.13, 4.7.2.6, page 219 - 226
