1-(甲基氨基)-3-苯基-2-丙炔合成路线 (共 10 条)
反应条件
sodium tetrahydroborate in ethanol Ambient temperature;
参考文献
Nussbaumer; Baumann; Dechat; Harasek
Tetrahedron, 1991 , vol. 47, # 26 p. 4591 - 4602
反应条件
copper(l) iodide; potassium carbonate; Tedicyp; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=80°C; 20 h;
参考文献
Lemhadri, Mhamed; Doucet, Henri; Santelli, Maurice
Synthesis, 2005 , # 8 art. no. Z22104SS, p. 1359 - 1367
反应条件
potassium hydrogencarbonate; copper(l) iodide in water; dimethyl sulfoxide T=30°C; 20 h;
参考文献
Bieber, Lothar W.; Da Silva, Margarete F.
Tetrahedron Letters, 2004 , vol. 45, # 45 p. 8281 - 8283
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane T=20°C; 6 h; Inert atmosphere;
参考文献
Gainer, Morgan J.; Bennett, Nitasha R.; Takahashi, Yu; Looper, Ryan E.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 3 p. 684 - 687
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in diethylamine
参考文献
Nomak, Rana; Snyder, John K.
Tetrahedron Letters, 2001 , vol. 42, # 45 p. 7929 - 7933
反应条件
1: 74 percent / ZnCl2 / dioxane / 2.5 h / Heating 2: 82 percent / TEA / CH2Cl2 / 1 h / Ambient temperature 3: 98 percent / NaBH4 / ethanol / Ambient temperature View Scheme
参考文献
Yang, Miao; Odelberg, Shannon J.; Tong, Zongzhong; Li, Dean Y.; Looper, Ryan E.
Tetrahedron, 2013 , vol. 69, # 27-28 p. 5744 - 5750
反应条件
1: 82 percent / TEA / CH2Cl2 / 1 h / Ambient temperature 2: 98 percent / NaBH4 / ethanol / Ambient temperature View Scheme
参考文献
Yang, Miao; Odelberg, Shannon J.; Tong, Zongzhong; Li, Dean Y.; Looper, Ryan E.
Tetrahedron, 2013 , vol. 69, # 27-28 p. 5744 - 5750
反应条件
Sonogashira Cross-Coupling;
参考文献
Hase, Shun; Kayaki, Yoshihito; Ikariya, Takao
Organometallics, 2013 , vol. 32, # 19 p. 5285 - 5288
参考文献
Babayan,A.T. et al.
Zhurnal Organicheskoi Khimii, 1973 , vol. 9, p. 467 - 471,472 - 476
反应条件
SCl2 in chloroform 24 h;
参考文献
Lendel, V. G.; Pak, V. I.; Petrus, V. V.; Kiyak, M. Yu.; Migalina, Yu. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 10 p. 1106 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 10 p. 1331 - 1334