3-羟基-5,5-二甲基环己-2-烯-1-酮合成路线 (共 39 条)
反应条件
sulfuryl dichloride in chloroform
2 h; Ambient temperature;
参考文献
Schank, Kurt; Blattner, Rudolf; Bouillon, Guenter
Chemische Berichte, 1981 , vol. 114, # 5 p. 1951 - 1957
反应条件
selenium(IV) oxide in methanol
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
acetic acid in acetonitrile
5 h; Heating;
参考文献
Singh, Kamaljit; Singh, Jasbir; Singh, Harjit
Tetrahedron, 1996 , vol. 52, # 45 p. 14273 - 14280
反应条件
piperidine in acetonitrile
2 h; Reflux;
参考文献
Rostamnia, Sadegh; Xin, Hongchuan; Liu, Xiao; Lamei, Kamran
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 374-375, p. 85 - 93
反应条件
sodium hydroxide; toluene-4-sulfonic acid in water
参考文献
Tochtermann, Werner; Koehn, Heinke
Chemische Berichte, 1980 , vol. 113, # 10 p. 3249 - 3261
反应条件
oxygen O2, singlet; tetrabutyl ammonium fluoride; methylene blue in ethanol
11 h; Irradiation;
参考文献
Wasserman, Harry H.; Pickett, James E.
Tetrahedron, 1985 , vol. 41, # 11 p. 2155 - 2162
反应条件
1: AcOH / propan-2-ol / 0.67 h / Heating
2: propan-2-ol / Heating
View Scheme
参考文献
Kolos; Yurchenko; Orlov; Shishkina; Shishkin
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 12 p. 1550 - 1559
反应条件
2-(tert-butyl)-1,1,3,3-tetramethylguanidine in benzene
T=60°C;
参考文献
Barton, Derek H. R.; Charpiot, Brigitte; Motherwell, William B.
Tetrahedron Letters, 1982 , vol. 23, # 33 p. 3365 - 3368
反应条件
2-(tert-butyl)-1,1,3,3-tetramethylguanidine in benzene
T=60°C;
参考文献
Barton, Derek H. R.; Charpiot, Brigitte; Motherwell, William B.
Tetrahedron Letters, 1982 , vol. 23, # 33 p. 3365 - 3368
反应条件
2-(tert-butyl)-1,1,3,3-tetramethylguanidine in benzene
T=60°C;
参考文献
Barton, Derek H. R.; Charpiot, Brigitte; Motherwell, William B.
Tetrahedron Letters, 1982 , vol. 23, # 33 p. 3365 - 3368