6-氯-1-三甲基甲硅烷基氧基己烷合成路线 (共 6 条)
反应条件
triethylamine in diethyl ether 0.25 h;
参考文献
Cloux, Roland; Schlosser, Manfred
Helvetica Chimica Acta, 1984 , vol. 67, p. 1470 - 1474
反应条件
in benzene 1.) 1.5 h, 60 deg C, 2.) light petroleum, 12 h;
参考文献
Caplin, Joseph; Tyman, John H. P.
Journal of Chemical Research, Miniprint, 1982 , # 2 p. 321 - 351
反应条件
1: 66 percent / conc. HCl, CuCl / toluene / 24 h / 100 °C 2: 88 percent / benzene / 1.) 1.5 h, 60 deg C, 2.) light petroleum, 12 h View Scheme
参考文献
Caplin, Joseph; Tyman, John H. P.
Journal of Chemical Research, Miniprint, 1982 , # 2 p. 321 - 351
反应条件
T=20°C; immediate distillation; Yield given;
参考文献
Kvicalova, Magdalena; Cermak, Jan; Blechta, Vratislav; Schraml, Jan
Collection of Czechoslovak Chemical Communications, 1997 , vol. 62, # 5 p. 816 - 820
参考文献
White,E. et al.
Journal of Organic Chemistry, 1970 , vol. 35, p. 4241 - 4244
反应条件
in cyclohexane; argon
参考文献
FMC Corporation
Patent: US5403946 A1, 1995 ;