反应条件
1: 1,3,5,7-cyclooctatetraene With lithium in diethyl ether T=25°C; 45 h; Inert atmosphere; 2: N,N-dimethylcarbamoyl chloride in diethyl ether T=0°C; Inert atmosphere; 3: With sulfuric acid in diethyl ether; water T=0°C;
参考文献
ANADYS PHARMACEUTICALS, INC.; WEBBER, Stephen, E.; TRAN, Chinh, V.; XIANG, Alan, Xin; MURPHY, Douglas, E.
Patent: WO2012/158271 A1, 2012 ;
Location in patent: Page/Page column 88-89 ;
