2-乙炔-4,4,5,5-四甲基-[1,3,2]二噁硼烷合成路线 (共 17 条)
反应条件
chloro-trimethyl-silane in acetone T=20°C;
参考文献
Geny, Anais; Lebaeuf, David; Rouquie, Gabriel; Vollhardt, K. Peter C.; Malacria, Max; Gandon, Vincent; Aubert, Corinne
Chemistry - A European Journal, 2007 , vol. 13, # 19 p. 5408 - 5425
参考文献
Kim, Mansuk; Lee, Daesung
Organic Letters, 2005 , vol. 7, # 9 p. 1865 - 1868
反应条件
in 1,2-dichloro-benzene T=190°C; 4 h; Inert atmosphere;
参考文献
Delaney, Patrick M.; Huang, Jianhui; Macdonald, Simon J. F.; Harrity, Joseph P. A.
Organic Letters, 2008 , vol. 10, # 5 p. 781 - 783
反应条件
in diphenylether T=170°C; 15 h;
参考文献
Tetrahedron, , vol. 64, # 5 p. 866 - 873
Chemical Communications, , # 31 p. 3323 - 3325
反应条件
in 1,2-dichloro-benzene T=180°C; 18 h;
参考文献
Tetrahedron, , vol. 64, # 5 p. 866 - 873
反应条件
in diphenylether T=170°C; 15 h; Title compound not separated from byproducts.;
参考文献
Tetrahedron, , vol. 64, # 5 p. 866 - 873
反应条件
in diphenylether T=170°C; 15 h;
参考文献
Delaney, Patrick M.; Moore, Jane E.; Harrity, Joseph P. A.
Chemical Communications, 2006 , # 31 p. 3323 - 3325
反应条件
in 1,2-dichloro-benzene T=180°C; 18 h;
参考文献
Delaney, Patrick M.; Browne, Duncan L.; Adams, Harry; Plant, Andrew; Harrity, Joseph P.A.
Tetrahedron, 2008 , vol. 64, # 5 p. 866 - 873
反应条件
in diphenylether T=170°C; 15 h; Title compound not separated from byproducts.;
参考文献
Delaney, Patrick M.; Browne, Duncan L.; Adams, Harry; Plant, Andrew; Harrity, Joseph P.A.
Tetrahedron, 2008 , vol. 64, # 5 p. 866 - 873
反应条件
in toluene T=110°C; 48 h; Inert atmosphere; regioselective reaction;
参考文献
Delaney, Patrick M.; Huang, Jianhui; Macdonald, Simon J. F.; Harrity, Joseph P. A.
Organic Letters, 2008 , vol. 10, # 5 p. 781 - 783