1-甲基-2-苯基-1H-咪唑合成路线 （共 22 条）
反应条件
18-crown-6 ether; potassium carbonate T=100°C; 10 h;
参考文献
Lissel, Manfred
Liebigs Annalen der Chemie, 1987 , p. 77 - 80
反应条件
1: 4,5-diiodo-1-methyl-2-phenyl-1H-imidazole With isopropylmagnesium chloride in tetrahydrofuran T=20°C; 1 h; 2: benzaldehyde in tetrahydrofuran T=-78 - 20°C; Further stages.;
参考文献
Butz, Ralf H.-J.; Lindell, Stephen D.
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2699 - 2701
反应条件
1: CuCl / 8 h / 85 °C 2: HCl / methanol / 4 h / Heating View Scheme
参考文献
Frutos, Rogelio P.; Gallou, Isabelle; Reeves, Diana; Xu, Yibo; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.
Tetrahedron Letters, 2005 , vol. 46, # 48 p. 8369 - 8372
反应条件
chloro-trimethyl-silane; ethylene dibromide; zinc; bis(dibenzylideneacetone)-palladium(0) 1.) THF, room temperature, 1 h, 2.) THF, 25 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Prasad, A. S. Bhanu; Stevenson, Thomas M.; Citineni, Janakiram Rao; Nyzam, Valerie; Knochel, Paul
Tetrahedron, 1997 , vol. 53, # 21 p. 7237 - 7254
反应条件
1: 2.) sodium perchlorate / 1.) 20-25 deg C, 24 h, 2.) methanol, water 2: 0.01M sodium hydroxide / ethanol; H2O / 0.17 h / Heating View Scheme
参考文献
Smolii, O. B.; Brovarets, V. S.; Pirozhenko, V. V.; Drach, B. S.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 12 p. 2635 - 2643,2345 - 2352
反应条件
in methanol Rearrangement; 2 h; Photolysis;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
反应条件
Methylation; 0.666667 h; room temperature -> steam bath;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
参考文献
Lawson
Journal of the Chemical Society, 1957 , p. 4225,4227
参考文献
Balaban; King
Journal of the Chemical Society, 1925 , vol. 127, p. 2710
反应条件
in methanol Rearrangement; ring cleavage; Photolysis; Quantum yieldKinetics;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
