1,2,3,4-四氢喹喔啉合成路线 （共 34 条）
反应条件
hydrogen bromide T=140°C; 24 h; sealed ampul;
参考文献
Gall', A. A.; Shishkin, G. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 5 p. 549 - 553
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 5 p. 677 - 681
反应条件
hydrogen bromide 2 h; Heating;
参考文献
Doronina, S. O.; Gall', A. A.; Shishkin, G. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 8 p. 897 - 900
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , # 8 p. 1117 - 1120
反应条件
n-ethyl morpholine; lithium aluminium tetrahydride P=14 Torr;
参考文献
Australian Journal of Chemistry, , vol. 9, p. 397,402
反应条件
1: 75 percent / dimethyl sulfoxide (DMSO), pyridine, trifluoroacetic acid, N,N'-dicyclohexylcarbodiimide / benzene / 72 h / Ambient temperature 2: 61 percent / conc. HBr / 2 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 27, # 8 p. 897 - 900
Khimiya Geterotsiklicheskikh Soedinenii, , # 8 p. 1117 - 1120
反应条件
1: 15 percent / KOH / aq. ethanol / 3 h / Heating 2: 1) 48percent HBr, 2) PBr3 / 1) ether, 2) sulfolane, 140 degC, 30 min 3: 48 percent / 48percent HBr / 60 h / 140 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 16, # 6 p. 648 - 653
Khimiya Geterotsiklicheskikh Soedinenii, , # 6 p. 831 - 836
反应条件
1: triethylamine / N,N-dimethyl-formamide / 36 h / 120 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 80 °C View Scheme
反应条件
hydrogenchloride; tin(ll) chloride Erwaermen des Reaktionsprodukts in Aethanol;
参考文献
Journal of the Chemical Society, , p. 4406,4408
反应条件
1: 1) 48percent HBr, 2) PBr3 / 1) ether, 2) sulfolane, 140 degC, 30 min 2: 48 percent / 48percent HBr / 60 h / 140 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 16, # 6 p. 648 - 653
Khimiya Geterotsiklicheskikh Soedinenii, , # 6 p. 831 - 836
反应条件
1: butan-1-ol 2: Na2S2; H2O 3: concentrated aqueous HCl / 150 - 160 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 4406,4408
参考文献
Chemische Berichte, , vol. 20, p. 1196
