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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
34793-63-0
合成路线
（共 7 条）
51118-07-1
→
反应条件
34793-63-0
反应条件
manganese(IV) oxide in diethyl ether T=20°C; 12 h;
参考文献
Auffrant, Audrey; Diederich, Francois; Boudon, Corinne; Gisselbrecht, Jean-Paul; Gross, Maurice
Helvetica Chimica Acta, 2004 , vol. 87, # 12 p. 3085 - 3105
107-31-3
甲酸甲酯
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
34793-63-0
反应条件
1: 4-ethynyl-1-methoxy-benzene With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.25 h; Inert atmosphere; 2: formic acid methyl ester in tetrahydrofuran; hexane T=0 - 20°C; 2.08333 h; Inert atmosphere;
参考文献
Qiu, Yi-Feng; Yang, Fang; Qiu, Zi-Hang; Zhong, Mei-Jin; Wang, Li-Jing; Ye, Yu-Ying; Song, Bo; Liang, Yong-Min
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12018 - 12028
768-60-5
4-乙炔基苯甲醚
→
反应条件
34793-63-0
反应条件
1.1: EtMgBr / tetrahydrofuran; diethyl ether / 1.5 h / 45 °C 1.2: 59 percent / tetrahydrofuran; diethyl ether / 5 h / 0 - 20 °C 2.1: 94 percent / MnO2 / diethyl ether / 12 h / 20 °C View Scheme
参考文献
Mueller,E.; Segnitz,A.
Justus Liebigs Annalen der Chemie, 1973 , p. 1583 - 1591
696-62-8
4-碘苯甲醚
→
反应条件
34793-63-0
反应条件
1.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 0.17 h / 20 °C / |Inert atmosphere 1.2: |Inert atmosphere 2.1: manganese(IV) oxide / dichloromethane / 20 °C 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 0 °C / |Inert atmosphere 3.2: |Inert atmosphere 4.1: manganese(IV) oxide / dichloromethane / 20 °C View Scheme
参考文献
Qiu, Yi-Feng; Yang, Fang; Qiu, Zi-Hang; Zhong, Mei-Jin; Wang, Li-Jing; Ye, Yu-Ying; Song, Bo; Liang, Yong-Min
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12018 - 12028
37614-59-8
3-(4-甲氧基苯基)-2-丙炔-1-醇
→
反应条件
34793-63-0
反应条件
1.1: manganese(IV) oxide / dichloromethane / 20 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 0 °C / |Inert atmosphere 2.2: |Inert atmosphere 3.1: manganese(IV) oxide / dichloromethane / 20 °C View Scheme
参考文献
Qiu, Yi-Feng; Yang, Fang; Qiu, Zi-Hang; Zhong, Mei-Jin; Wang, Li-Jing; Ye, Yu-Ying; Song, Bo; Liang, Yong-Min
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12018 - 12028
90696-21-2
→
反应条件
34793-63-0
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 0 °C / |Inert atmosphere 1.2: |Inert atmosphere 2.1: manganese(IV) oxide / dichloromethane / 20 °C View Scheme
参考文献
Qiu, Yi-Feng; Yang, Fang; Qiu, Zi-Hang; Zhong, Mei-Jin; Wang, Li-Jing; Ye, Yu-Ying; Song, Bo; Liang, Yong-Min
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12018 - 12028
34793-63-0
→
反应条件
22779-05-1
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2; chlorobenzene T=90 - 140°C; 24.5 h; Inert atmosphere;
参考文献
Dermenci, Alpay; Whittaker, Rachel E.; Dong, Guangbin
Organic Letters, 2013 , vol. 15, # 9 p. 2242 - 2245
