N-(2-吡啶基)甲酰胺合成路线 (共 29 条)
反应条件
tri-ruthenium(0)dodecacarbonyl in acetonitrile 2 h; Heating;
参考文献
Ko, Sangwon; Han, Hoon; Chang, Sukbok
Organic Letters, 2003 , vol. 5, # 15 p. 2687 - 2690
反应条件
1: chloroform / unter Druck 2: aqueous K2CO3 View Scheme
参考文献
Schilling et al.
Chemische Berichte, 1955 , vol. 88, p. 1093,1100
反应条件
1: 1.) NaH / 1.) toluene, 2.) 40 h, 50 deg C 2: 56 percent / 96percent formic acid / 5 h / Heating View Scheme
参考文献
Reisch, Johannes; Scheer, Mathias
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 2 p. 677 - 679
参考文献
Kawasaki, Motoji; Suzuki, Yasutaka; Terashima, Shiro
Chemistry Letters, 1984 , p. 239 - 242
反应条件
1: N-(pyridin-2-yl)formamide With trichlorophosphate T=80°C; 2 h; 2: N,N-dimethyl-aniline T=90°C; 18 h; Further stages.;
参考文献
Cheng, Ying; Jiao, Peng; Williams, David J.; Cohn, Otto-Meth
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 1 p. 44 - 46
反应条件
sodium hydrogencarbonate; tri-ruthenium(0)dodecacarbonyl; palladium dichloride in acetonitrile T=135°C; 8 h;
参考文献
Ko, Sangwon; Han, Hoon; Chang, Sukbok
Organic Letters, 2003 , vol. 5, # 15 p. 2687 - 2690
反应条件
sodium hydrogencarbonate; tri-ruthenium(0)dodecacarbonyl; palladium dichloride in acetonitrile
T=135°C; 6 h;
参考文献
Ko, Sangwon; Han, Hoon; Chang, Sukbok
Organic Letters, 2003 , vol. 5, # 15 p. 2687 - 2690
反应条件
sodium hydride in N,N-dimethyl-formamide
T=0 - 20°C; 1.5 h;
参考文献
Krein, Douglas M.; Lowary, Todd L.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4965 - 4967
参考文献
Kawasaki, Motoji; Suzuki, Yasutaka; Terashima, Shiro
Chemistry Letters, 1984 , p. 239 - 242