in dichloromethane
under N2; dissolved org. S-compound was cooled to 0°C; addn. of BF3-Et2O; stirred for 0.25 h; dropwise addn. of Fe-complex soln.; stirred for 4 h at 0°C; addn. of H2O; extn. (CH2Cl2); dried (MgSO4); solvent removal by evapn.; chromy. (silica gel; eluent: CH2Cl2/petroleum ether);;
参考文献
Powell, Kimberly R.; Elias, W. Jeff; Welker, Mark E.
Journal of Organometallic Chemistry, 1991 , vol. 407, # 1 p. 81 - 89
