2-甲基-6-硝基-1H-吲哚合成路线 (共 7 条)
反应条件
triethylamine; α-bromoacetophenone in methanol T=20°C; 3 h;
参考文献
Bujok, Robert; Wrbel, Zbigniew; Wojciechowski, Krzysztof
Synlett, 2012 , vol. 23, # 9 p. 1315 - 1320
反应条件
chloranil in xylene T=140°C; 2 h;
参考文献
Severino, Beatrice; Fiorino, Ferdinando; Perissutti, Elisa; Frecentese, Francesco; Cirino, Giuseppe; Roviezzo, Fiorentina; Santagada, Vincenzo; Caliendo, Giuseppe
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 11 p. 6009 - 6020
反应条件
air; potassium tert-butylate in dimethyl sulfoxide 2 h;
参考文献
Moskalev, Nikolai; Barbasiewicz, Michal; Makosza, Mieczyslaw
Tetrahedron, 2004 , vol. 60, # 2 p. 347 - 358
反应条件
air; potassium tert-butylate in dimethyl sulfoxide 2 h;
参考文献
Moskalev, Nikolai; Barbasiewicz, Michal; Makosza, Mieczyslaw
Tetrahedron, 2004 , vol. 60, # 2 p. 347 - 358
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / -20 - 20 °C 2: tin(ll) chloride / ethanol; ethyl acetate / 20 °C 3: triethylamine; α-bromoacetophenone / methanol / 3 h / 20 °C View Scheme
参考文献
Bujok, Robert; Wrbel, Zbigniew; Wojciechowski, Krzysztof
Synlett, 2012 , vol. 23, # 9 p. 1315 - 1320
反应条件
1: tin(ll) chloride / ethanol; ethyl acetate / 20 °C 2: triethylamine; α-bromoacetophenone / methanol / 3 h / 20 °C View Scheme
参考文献
Bujok, Robert; Wrbel, Zbigniew; Wojciechowski, Krzysztof
Synlett, 2012 , vol. 23, # 9 p. 1315 - 1320
反应条件
ethanol; nickel; hydrazine hydrate
参考文献
Terent'ew et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2541,2550; engl. Ausg. S. 2504, 2511