hydrogen; lithium aluminium tetrahydride; titanium tetrachloride in n-heptane T=200°C; P=67505.4 Torr; 3 h; Further byproducts given;

white sand; calcium; tert-butyl alcohol in tetrahydrofuran; ethylenediamine T=0°C; 24 h; Yield given;

calcium shot; ethylenediamine; methylamine 42 h;

hydrogen; lithium aluminium tetrahydride; titanium tetrachloride in n-heptane T=200°C; P=67505.4 Torr; 3 h; other conditions: other solvents (diglyme, nonane, hexane), other times, other catalysts, other reagents (D2O, H2O/LiAlD4), other temperatures;; Product distribution;

tetra(n-butyl)ammonium hydroxide in water T=80°C; electrolysis, 10 F/mol, divided cell;

Wilkinson's catalyst; hydrogen

Yield given. Multistep reaction;

1.) electrolysis, 2.1M tetrabutylammonium hydroxide, 80 deg C, 2.) reflux, 48 h; different electrolytic cells; Product distribution;