4-硝基-4’-叔丁基二苯醚合成路线 (共 12 条)
反应条件
potassium carbonate in dimethyl sulfoxide Ullmann Condensation; 4 h;
参考文献
Singh, Abhilash S.; Shendage, Suresh S.; Nagarkar, Jayashree M.
Tetrahedron Letters, 2013 , vol. 54, # 47 p. 6319 - 6323
反应条件
potassium fluoride supported on Clinoptilolite in dimethyl sulfoxide T=110 - 115°C; 1.33333 h;
参考文献
Khalilzadeh, Mohammad A.; Hosseini, Abolfazl; Pilevar, Afsaneh
European Journal of Organic Chemistry, 2011 , # 8 p. 1587 - 1592
反应条件
copper(l) iodide; glycine-N',N'-dimethylamide hydrochloride; caesium carbonate in 1,4-dioxane T=90°C; Ullmann coupling reaction; 20 h;
参考文献
Ma, Dawei; Cai, Qian
Organic Letters, 2003 , vol. 5, # 21 p. 3799 - 3802
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20°C; Substitution;
参考文献
Neuville, Luc; Bigot, Antony; Tran Huu Dau, Marie Elise; Zhu, Jieping
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7638 - 7642
反应条件
potassium carbonate in acetonitrile T=50°C; 24 h;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
carbon dioxide; tetrabutylammomium bromide; cesium fluoride T=90°C; P=157516 Torr; 16 h;
参考文献
Lee, Jin-Kyun; Fuchter, Matthew J.; Williamson, Rachel M.; Leeke, Gary A.; Bush, Edward J.; McConvey, Ian F.; Saubern, Simon; Ryan, John H.; Holmes, Andrew B.
Chemical Communications, 2008 , # 39 p. 4780 - 4782
反应条件
caesium carbonate in dimethyl sulfoxide 0.133333 h; microwave irradiation;
参考文献
Xu, Hui; Chen, Yang
Synthetic Communications, 2007 , vol. 37, # 14 p. 2411 - 2420
反应条件
nickel(II) ferrite; caesium carbonate in 1,4-dioxane 10 h; Reflux;
参考文献
Paul, Sanjay; Pradhan, Koyel; Ghosh, Sirshendu; De; Das, Asish R.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 6 p. 1301 - 1316
反应条件
1: 90 percent / Et3N / CH2Cl2 / 12 h / 20 °C 2: 28 percent / Cs2CO3 / dimethylformamide / 20 °C View Scheme
参考文献
Neuville, Luc; Bigot, Antony; Tran Huu Dau, Marie Elise; Zhu, Jieping
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7638 - 7642
反应条件
1: iodine; dipotassium peroxodisulfate 2: potassium carbonate / acetonitrile / 24 h / 50 °C View Scheme
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188