2-丁氧基-1,3,2-苯并二氧硼烷合成路线 (共 13 条)
反应条件
in toluene 17 h; Heating;
参考文献
Pineschi, Mauro; Bertolini, Ferruccio; Haak, Robert M.; Crotti, Paolo; Macchia, Franco
Chemical Communications, 2005 , # 11 p. 1426 - 1428
反应条件
1: CH2Cl2; BCl3 / -80 °C 2: CH2Cl2 View Scheme
参考文献
Gerrard et al.
Journal of the Chemical Society, 1959 , p. 1529,1531, 1533
参考文献
Gerrard et al.
Journal of the Chemical Society, 1959 , p. 1529,1531, 1533
参考文献
Gerrard et al.
Journal of the Chemical Society, 1959 , p. 1529,1531, 1533
参考文献
Gerrard et al.
Journal of the Chemical Society, 1959 , p. 1529,1531, 1533
参考文献
Lappert,M.F. et al.
Journal of the Chemical Society, 1965 , p. 4256 - 4264
参考文献
Journal of the Chemical Society, , p. 1529 - 1535
B: B-Verb.9, 3.2.6, page 67 - 74
反应条件
in benzene to benzene soln. of nitrone of salicylaldehyde added (C6H4O2)BOC4H9 (molar ratio 1:1), refluxed for 30 min; concd. in vac., added petroleum ether, ppt. washed with ether, dried, elem. anal.;
参考文献
Kliegel, Wolfgang; Nanninga, Dierk
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 373 - 386
反应条件
in benzene to benzene soln. of nitrone of salicylaldehyde added (C6H4O2)BOC4H9 (molar ratio 1:1), refluxed for 30 min; concd. in vac., added petroleum ether, ppt. recrystd. from benzene/petroleum ether, dried, elem. anal.;
参考文献
Kliegel, Wolfgang; Nanninga, Dierk
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 373 - 386
反应条件
in benzene to benzene soln. of nitrone of salicylaldehyde added (C6H4O2)BOC4H9 (molar ratio 1:1), refluxed for 30 min; concd. in vac., added petroleum ether, ppt. washed with ether, dried, elem. anal.;
参考文献
Kliegel, Wolfgang; Nanninga, Dierk
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 373 - 386