1-甲氧基-1-三甲基硅氧基丙烯合成路线 （共 16 条）
反应条件
titanium(IV) isopropylate; titanium tetrachloride
1.) CH2Cl2, -78 deg C, 1 h, 0 deg C, 2 h; 2.) H2O, DME, heating, 3 h; Yield given. Multistep reaction;
参考文献
Miyashita; Yanami; Kumazawa; Yoshikoshi
Journal of the American Chemical Society, 1984 , vol. 106, # 7 p. 2149 - 2156
反应条件
titanium(IV) isopropylate; titanium tetrachloride; ethylene glycol dimethyl ether
1) dichloromethane, -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Miyashita, Masaaki; Kumazawa, Toshiaki; Yoshikoshi, Akira
Chemistry Letters, 1980 , p. 1043 - 1044
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
3.5 h; Ambient temperature;
参考文献
Ikeda, Kiyoshi; Achiwa, Kazuo; Sekiya, Minoru
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4707 - 4710
反应条件
zinc(II) chloride in dichloromethane
6 h; Heating;
参考文献
Tanimoto, Shigeo; Ikehira, Hideyuki; Oida, Tatsuo; Kokubo, Toshio
Synthesis, 1983 , # 10 p. 787 - 788
反应条件
in benzene
8.5 h; PhotolysisInert atmosphere; regioselective reaction;
参考文献
Cho, Dae Won; Park, Hea Jung; Yoon, Ung Chan; Lee, Hyang-Yeol; Mariano, Patrick S.
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10304 - 10313
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 2 h;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
