2-羟基-4-甲氧基-6-甲基苯甲醛合成路线 (共 7 条)
反应条件
potassium carbonate in acetone 5 h; Reflux;
参考文献
Merck Patent GmbH
Patent: US2010/16372 A1, 2010 ;
Location in patent: Page/Page column 12 ;
US 20100016372 A1
反应条件
boron trichloride in dichloromethane
参考文献
Sargent, Melvyn V.; Stransky, Peter O.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2373 - 2378
反应条件
1: phosphoryl chloride / 15 h / Ambient temperature 2: 22.4 g / boron trichloride / CH2Cl2 / 2 h / -10 °C View Scheme
参考文献
Sargent, Melvyn V.; Stransky, Peter O.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2373 - 2378
反应条件
hydrogenchloride; benzene in der Kaelte,Zufuegen von Aluminiumchlorid und nochmaligen Einleiten von Chlorwasserstoff bei 40grad;
参考文献
Pfau
Helvetica Chimica Acta, 1928 , vol. 11, p. 873
反应条件
sodium hydroxide; acetone
参考文献
Hoesch
Chemische Berichte, 1913 , vol. 46, p. 887
反应条件
hydrogenchloride; mercury dichloride; zinc in ethanol
参考文献
Witty,T.R.; Remers,W.A.
Journal of Medicinal Chemistry, 1973 , vol. 16, p. 1280 - 1284
参考文献
Hoesch
Chemische Berichte, 1913 , vol. 46, p. 887