苄氧羰基-alpha-苄基-gamma-琥珀酰亚胺基-L-谷氨酸酯合成路线 (共 3 条)
反应条件
dicyclohexyl-carbodiimide in 1,4-dioxane T=4°C; 12 h;
参考文献
Verbruggen, Christophe; De Craecker, Sofie; Rajan, Padinchare; Jiao, Xian-Yun; Borloo, Marianne; Smith, Keith; Fairlamb, Alan H.; Haemers, Achiel
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 3 p. 253 - 258
反应条件
dicyclohexyl-carbodiimide; citric acid 1) EtOAc, 2) EtOAc, RT, 15 h; Yield given. Multistep reaction;
参考文献
Pettit, Georeg R.; Nelson, Paul S.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2097 - 2102
反应条件
1: Et3N / dimethylformamide; H2O / 24 h / Ambient temperature 2: 84 percent / H2 / Pd black / aq. acetic acid; methanol / 5 h View Scheme
参考文献
Noda, Kosaku; Igata, Keiko; Horikawa, Yoshiko; Fujii, Hisao
Agricultural and Biological Chemistry, 1980 , vol. 44, # 10 p. 2419 - 2424