3-甲氧基-5-三氟甲基苯胺合成路线 （共 10 条）
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran T=20°C; 12 h;
参考文献
Rahaim Jr., Ronald J.; Maleczka Jr., Robert E.
Synthesis, 2006 , # 19 p. 3316 - 3340
反应条件
1: methanol 2: iron View Scheme
参考文献
Journal of the American Chemical Society, , vol. 77, p. 2284,2285
反应条件
ammonia; sodium amide
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3011,3012
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3011,3012
反应条件
sodium nitrite in hydrogenchloride; water
参考文献
Tanabe Seiyaku Co., Ltd.
Patent: US6521666 B1, 2003 ;
参考文献
Altmann, Karl-Heinz; Bold, Guido; Furet, Pascal; Manley, Paul William; Wood, Jeanette Marjorie; Ferrari, Stefano; Hofmann, Francesco; Mestan, Jurgen; Huth, Andreas; Kruger, Martin; Seidelmann, Dieter; Menrad, Andreas; Haberey, Martin; Thierauch, Karl-Heinz
Patent: US2002/19414 A1, 2002 ;
反应条件
1: With hydrogenchloride; trifluoroacetic acid; sodium nitrite in water T=0°C; 2: With sulfur dioxide; anhydrous sulfurous acid; acetic acid; copper(l) chloride; copper dichloride in water T=0 - 20°C;
参考文献
US2010/41713 A1, ;
Page/Page column 21 ;
US 20100041713 A1
参考文献
Boehringer Ingelheim GmbH
Patent: US4058642 A1, 1977 ;
反应条件
in acetonitrile
T=25°C; Kinetics;
参考文献
Emokpae,T.A.; Dosunma,I.M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1977 , p. 14 - 17
反应条件
sulfuric acid; hydrogen bromide; copper(I) bromide; sodium nitrite in acetic acid
T=0 - 20°C;
参考文献
MacDonald, Gregor James; Thuring, Johannes Wilhelmus John F.; Van den Keybus, Frans Alfons Maria; Van Roosbroeck, Yves Emiel Maria
Patent: US2012/172354 A1, 2012 ;
Location in patent: Page/Page column 17 ;
