3,5-二(三氟甲基)苯乙烯合成路线 （共 8 条）
反应条件
tetrabutyl-ammonium chloride; triethylamine; palladium diacetate in acetonitrile T=80°C; P=49130.4 Torr; 36 h;
参考文献
Chemistry - A European Journal, , vol. 8, # 6 p. 1372 - 1376
反应条件
tetrafluoroboric acid in dichloromethane; cyclohexane T=-17 - 5°C; 23.6667 h;
参考文献
US2007/15923 A1, ;
Page/Page column 14; 15 ;
反应条件
phosphorus pentoxide; hydroquinone; benzene
参考文献
Journal of the American Chemical Society, , vol. 72, p. 4053
反应条件
1: magnesium / tetrahydrofuran 2: phosphorous pentoxide View Scheme
参考文献
Polymer, , vol. 52, # 4 p. 949 - 953
反应条件
triethylamine Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 71, # 19 p. 7378 - 7390
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tortolani, David R.; Biller, Scott A.
Tetrahedron Letters, 1996 , vol. 37, # 32 p. 5687 - 5690
反应条件
dichloro bis(acetonitrile) palladium(II); [Ph4(η5-C4CO)2H(CO)4Ru2](μ-H); water; p-benozquinone in methanol; isopropyl alcohol
T=85°C; 36 h; Inert atmosphereGlovebox; regioselective reaction;
参考文献
Yang, Yongsheng; Guo, Jiayi; Ng, Huimin; Chen, Zhiyong; Teo, Peili
Chemical Communications, 2014 , vol. 50, # 20 p. 2608 - 2611
反应条件
dichloro bis(acetonitrile) palladium(II); (Ru2(η5-C5Ph4O)2(H)2(CO)4); water; isopropyl alcohol; p-benozquinone; copper dichloride; tert-butyl alcohol
T=85°C;
参考文献
Dong, Guangbin; Teo, Peili; Wickens, Zachary K.; Grubbs, Robert H.
Science, 2011 , vol. 333, # 6049 p. 1609 - 1612
