2-苯氧基-1,4-苯醌合成路线 （共 13 条）
反应条件
potassium fluoride in N,N-dimethyl-formamide T=90°C;
参考文献
Rao, A. V. Rama; Gurjar, Mukund K.; Reddy, A. Bhaskar; Khare, Vivek, B.
Tetrahedron Letters, 1993 , vol. 34, # 10 p. 1657 - 1660
反应条件
1.1: dimethylformamide / 0.33 h 1.2: dimethylformamide 2.1: concentrated HCl / methanol; H2O / 0.5 h 3.1: 70 percent / sodium borohydride / aq. ethanol / 0.17 h 4.1: hydrogen / 30percent Pd/C / methanol / 3.5 h 5.1: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C View Scheme
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
1.1: dimethylformamide / 0.33 h 1.2: dimethylformamide 2.1: concentrated HCl / methanol; H2O / 0.5 h 3.1: 70 percent / sodium borohydride / aq. ethanol / 0.17 h 4.1: hydrogen / 30percent Pd/C / methanol / 3.5 h 5.1: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C View Scheme
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
1.1: dimethylformamide / 0.33 h 1.2: dimethylformamide 2.1: concentrated HCl / methanol; H2O / 0.5 h 3.1: 70 percent / sodium borohydride / aq. ethanol / 0.17 h 4.1: hydrogen / 30percent Pd/C / methanol / 3.5 h 5.1: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C View Scheme
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
1: 40 percent Chromat. / calcium hypochlorite / dimethylformamide / 0.33 h 2: 70 percent / sodium borohydride / aq. ethanol / 0.17 h 3: hydrogen / 30percent Pd/C / methanol / 3.5 h 4: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C View Scheme
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
1: 70 percent / sodium borohydride / aq. ethanol / 0.17 h 2: hydrogen / 30percent Pd/C / methanol / 3.5 h 3: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C View Scheme
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
1: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C 2: hydrogen / 30percent Pd/C / methanol / 4.5 h 3: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C View Scheme
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
1: concentrated HCl / methanol; H2O / 0.5 h 2: 70 percent / sodium borohydride / aq. ethanol / 0.17 h 3: hydrogen / 30percent Pd/C / methanol / 3.5 h 4: CrO3; acetic acid / H2O / 0.33 h / 0 - 10 °C View Scheme
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
chromium(VI) oxide; acetic acid in water T=0 - 10°C; 0.333333 h;
参考文献
Heasley, Victor L.; Anderson, James D.; Bowman, Zachery S.; Hanley Jr., John C.; Sigmund, Geoffery A.; Van Horn, David; Shellhamer, Dale F.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6827 - 6830
反应条件
potassium dichromate; sulfuric acid
参考文献
Ungnade; Zilch
Journal of Organic Chemistry, 1950 , vol. 15, p. 1108,1110
Journal of Organic Chemistry, 1951 , vol. 16, p. 64,69
