P,P′-(9,9-二甲基-9H-氧杂蒽-4,5-二基)双[N,N,N′,N′-四乙基-亚膦酸二酰胺]合成路线 (共 1 条)
反应条件
1: 9,9-dimethyl-9H-xanthene With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane T=-40 - 20°C; 2: bis(diethylamino)phosphorochloridite in diethyl ether; hexane; pentane T=-60 - 20°C; Further stages.;
参考文献
Van Der Vlugt, Jarl Ivar; Hewat, Alison C.; Neto, Samuel; Sablong, Rafael; Mills, Allison M.; Lutz, Martin; Spek, Anthony L.; Mueller, Christian; Vogt, Dieter
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 8 p. 993 - 1003