8-羟基-2-甲基喹啉-5-(N,N-二甲基)磺酰胺合成路线 (共 10 条)
反应条件
in tetrahydrofuran 3.16667 h;
参考文献
Shults, Melissa D.; Pearce, Dierdre A.; Imperiali, Barbara
Journal of the American Chemical Society, 2003 , vol. 125, # 35 p. 10591 - 10597
反应条件
1: 2.8 g / chlorosulfonic acid / 2 h / 25 °C 2: 45 percent / tetrahydrofuran / 25 °C View Scheme
参考文献
Yamaguchi, Tomoko; Watanabe, Shinya; Matsumura, Yuriko; Tokuoka, Yoshikazu; Yokoyama, Akihiro
Chemical and Pharmaceutical Bulletin, 2012 , vol. 60, # 4 p. 508 - 512
反应条件
sodium nitrate; water; 2-[4-(2-hydroxyethyl)-1-piperazinyl] ethanesulfonic acid in acetonitrile T=25°C; pH=7.4; UV-irradiation;
参考文献
Aoki, Shin; Matsuo, Nanako; Hanaya, Kengo; Yamada, Yasuyuki; Kageyama, Yoshiyuki
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 9 p. 3405 - 3413
反应条件
sodium nitrate in water; acetonitrile T=25°C; pH=7.4; PhotolysisUV-irradiationHEPES buffer; Quantum yield;
参考文献
Ariyasu, Shinya; Hanaya, Kengo; Tsunoda, Megumi; Kitamura, Masanori; Hayase, Masanori; Abe, Ryo; Aoki, Shin
Chemical and Pharmaceutical Bulletin, 2011 , vol. 59, # 11 p. 1355 - 1362
反应条件
1: 2-methyl-8-hydroxyquinoline With chlorosulfonic acid 2: dimethyl amine
参考文献
Royzen, Maksim; Canary, James W.
Polyhedron, 2013 , vol. 58, p. 85 - 91
反应条件
triethylamine in acetonitrile T=25°C; pH=7.4; HEPES bufferUV-irradiationInert atmosphere; KineticsQuantum yield; Reagent/catalyst;
参考文献
Kageyama, Yoshiyuki; Ohshima, Ryosuke; Sakurama, Kazusa; Fujiwara, Yoshihisa; Tanimoto, Yoshifumi; Yamada, Yasuyuki; Aoki, Shin
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 11 p. 1257 - 1266
反应条件
in water-d2; acetonitrile-D3 T=25°C; pH=7.4; HEPES bufferUV-irradiationInert atmosphere; Quantum yield;
参考文献
Kageyama, Yoshiyuki; Ohshima, Ryosuke; Sakurama, Kazusa; Fujiwara, Yoshihisa; Tanimoto, Yoshifumi; Yamada, Yasuyuki; Aoki, Shin
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 11 p. 1257 - 1266
反应条件
in water-d2; acetonitrile-D3 T=25°C; pH=7.4; HEPES bufferUV-irradiationInert atmosphere; Quantum yield;
参考文献
Kageyama, Yoshiyuki; Ohshima, Ryosuke; Sakurama, Kazusa; Fujiwara, Yoshihisa; Tanimoto, Yoshifumi; Yamada, Yasuyuki; Aoki, Shin
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 11 p. 1257 - 1266
反应条件
in water-d2; acetonitrile-D3 T=25°C; pH=7.4; HEPES bufferUV-irradiationInert atmosphere; Quantum yield;
参考文献
Kageyama, Yoshiyuki; Ohshima, Ryosuke; Sakurama, Kazusa; Fujiwara, Yoshihisa; Tanimoto, Yoshifumi; Yamada, Yasuyuki; Aoki, Shin
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 11 p. 1257 - 1266
反应条件
in water-d2; acetonitrile-D3 T=25°C; pH=7.4; HEPES bufferUV-irradiationInert atmosphere; Quantum yield;
参考文献
Kageyama, Yoshiyuki; Ohshima, Ryosuke; Sakurama, Kazusa; Fujiwara, Yoshihisa; Tanimoto, Yoshifumi; Yamada, Yasuyuki; Aoki, Shin
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 11 p. 1257 - 1266