N-(2-溴苯基)-4-甲氧基苯甲酰胺合成路线 (共 6 条)
反应条件
1: para-iodoanisole; 1-Bromo-2-aminobenzene With palladium diacetate; triethylamine in water 0.166667 h; 2: carbon monoxide in water T=100°C; P=10343.2 Torr; 8 h;
参考文献
Tambade, Pawan J.; Patil, Yogesh P.; Qureshi, Ziyauddin S.; Dhake, Kishor P.; Bhanage, Bhalchandra M.
Synthetic Communications, 2012 , vol. 42, # 2 p. 176 - 185
反应条件
in tetrahydrofuran T=20°C; 24 h;
参考文献
Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 1802 - 1808
反应条件
palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane T=110°C; 1 h;
参考文献
Begouin, Agathe; Queiroz, Maria-Joao R. P.
European Journal of Organic Chemistry, 2009 , # 17 p. 2820 - 2827
参考文献
Itoh, Naoki; Sakamoto, Takeshi; Miyazawa, Etsuko; Kikugawa, Yasuo
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7424 - 7428
反应条件
1.1: i-Pr2NEt; xantphos / Pd2(dba)3 / dioxane / 12 h / Heating 2.1: NaOEt / tetrahydrofuran; ethanol / 1 h / 50 °C 2.2: trifluoroacetic acid / tetrahydrofuran; ethanol / Heating View Scheme
参考文献
Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 1802 - 1808
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in ethylene glycol dimethyl ether
24 h; Heating;
参考文献
Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 1802 - 1808