1-M乙烷磺酰基哌啶-3-羧酸乙酯合成路线 （共 5 条）
反应条件
triethylamine in dichloromethane T=0°C; 4 h;
参考文献
Chang, Meng-Yang; Lin, Chung-Han; Lee, Tein-Wei
Tetrahedron Letters, 2012 , vol. 53, # 6 p. 627 - 631
反应条件
1: With water; sodium hydroxide in methanol T=0 - 20°C; 6 h; 2: With hydrogenchloride in water pH=3;
参考文献
Dainippon Sumitomo Pharma Co., Ltd.; KISO, Yoshiaki
Patent: WO2007/29587 A1, 2007 ;
Location in patent: Page/Page column 67 ;
WO 2007/029587 A1
反应条件
1: lithium aluminum hydride / tetrahydrofuran / 5 h / 0 °C
2: pyridinium chlorochromate; Celite / CH2Cl2 / 5 h / 20 °C
3: tetrahydrofuran / 5 h / -78 °C
4: pyridinium chlorochromate; Celite / CH2Cl2 / 5 h / 20 °C
View Scheme
参考文献
Chang, Meng-Yang; Kung, Yung-Hua; Ma, Chih-Chong
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 199 - 202
反应条件
1: lithium aluminum hydride / tetrahydrofuran / 5 h / 0 °C
2: pyridinium chlorochromate; Celite / CH2Cl2 / 5 h / 20 °C
3: tetrahydrofuran / 5 h / -78 °C
4: pyridinium chlorochromate; Celite / CH2Cl2 / 5 h / 20 °C
View Scheme
参考文献
Chang, Meng-Yang; Kung, Yung-Hua; Ma, Chih-Chong
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 199 - 202
反应条件
1: lithium aluminum hydride / tetrahydrofuran / 5 h / 0 °C
2: pyridinium chlorochromate; Celite / CH2Cl2 / 5 h / 20 °C
3: tetrahydrofuran / 5 h / -78 °C
4: pyridinium chlorochromate; Celite / CH2Cl2 / 5 h / 20 °C
View Scheme
参考文献
Chang, Meng-Yang; Kung, Yung-Hua; Ma, Chih-Chong
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 199 - 202
