(2-氯苯基)氧代乙酸甲酯合成路线 (共 16 条)
反应条件
(hydroxy(tosyloxy)iodo)benzene 0.0833333 h; microwave irradiation;
参考文献
Lee, Jong Chan; Lee, Ji Young; Lee, Seung Jun
Tetrahedron Letters, 2004 , vol. 45, # 25 p. 4939 - 4941
反应条件
water; diethylazodicarboxylate; dirhodium tetraacetate in toluene 4 h; Heating;
参考文献
Guo, Zhenqiu; Huang, Haoxi; Fu, Qingquan; Hu, Wenhao
Synlett, 2006 , # 15 p. 2486 - 2488
反应条件
1: 1-bromo-2-chloro-benzene With iodine; magnesium in tetrahydrofuran T=10 - 15°C; 0.5 h; Inert atmosphere; 2: oxalic acid dimethyl ester in tetrahydrofuran; diethyl ether T=-70°C;
参考文献
Ema, Tadashi; Ide, Sayaka; Okita, Nobuyasu; Sakai, Takashi
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 2039 - 2044
反应条件
tert.-butylhydroperoxide; vanadium pillared montmorillonite catalyst (V-PILC) in methanol; 2,2,4-trimethylpentane T=70°C; 48 h;
参考文献
Choudary, B. M.; Reddy, G. Vidya Sagar; Rao, K. Koteswara
Journal of the Chemical Society, Chemical Communications, 1993 , # 3 p. 323 - 324
反应条件
1: 1-(2-chlorophenyl)ethan-1-one With pyridine; selenium(IV) oxide T=100°C; 15 h; Inert atmosphere; 2: methanol With thionyl chloride T=20°C; Cooling with iceMolecular sieve; 3: With perchloric acid; water in acetonitrile T=20°C; 0.5 h;
参考文献
Zhuang, Jing; Wang, Changqing; Xie, Fang; Zhang, Wanbin
Tetrahedron, 2009 , vol. 65, # 47 p. 9797 - 9800
反应条件
CuCl2·2H2O; 3-chloro-benzenecarboperoxoic acid in nitromethane T=60°C; 10 h;
参考文献
Liu, Jia; Zhu, Xiao-Rui; Ren, Jiangmeng; Chen, Wei-Dong; Zeng, Bu-Bing
Synlett, 2013 , vol. 24, # 20 art. no. ST-2013-W0735-L, p. 2740 - 2742
反应条件
2,4-bis(1,1-dimethylethyl)-6-({[(1S)-1-hydroxymethyl-2-methylpropyl]imino}methyl)phenol; oxygen; vanadium triisopropoxide oxide in acetone T=20°C; 12 h; optical yield given as percent eeenantioselective reaction;
参考文献
Yin, Lu; Jia, Xian; Li, Xing Shu; Chan, Albert S.C.
Chinese Chemical Letters, 2010 , vol. 21, # 7 p. 774 - 777
反应条件
C28H38N2O2; oxygen; vanadium triisopropoxide oxide in acetone T=20°C; 12 h; optical yield given as percent eeenantioselective reaction;
参考文献
Yin, Lu; Jia, Xian; Li, Xing Shu; Chan, Albert S.C.
Chinese Chemical Letters, 2010 , vol. 21, # 7 p. 774 - 777
反应条件
1: sulfuric acid; water 2: thionyl chloride View Scheme
参考文献
Veerareddy, Arava; Surendrareddy, Gogireddy; Dubey
Synthetic Communications, 2013 , vol. 43, # 16 p. 2236 - 2241
参考文献
Veerareddy, Arava; Surendrareddy, Gogireddy; Dubey
Synthetic Communications, 2013 , vol. 43, # 16 p. 2236 - 2241