4,4,5,5-四甲基-2-(芘-1-基)-1,3,2-二噁唑环戊硼烷合成路线 （共 15 条）
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene Suzuki cross-coupling; 48 h; Heating;
参考文献
Modrakowski; Flores; Beinhoff; Schlueter
Synthesis, 2001 , # 14 p. 2143 - 2155
反应条件
1.1: 91 percent / aq. Na2CO3 / Pd(PPh3)4 / toluene / 48 h / Heating
2.1: n-BuLi / tetrahydrofuran / 6 h / -78 - 20 °C
2.2: B(O-iPr)3 / tetrahydrofuran / 10 h / -78 - 20 °C
View Scheme
参考文献
Modrakowski; Flores; Beinhoff; Schlueter
Synthesis, 2001 , # 14 p. 2143 - 2155
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene
Suzuki cross-coupling; Heating;
参考文献
Beinhoff, Matthias; Weigel, Wilfried; Jurczok, Martin; Rettig, Wolfgang; Modrakowski, Claudia; Bruedgam, Irene; Hartl, Hans; Schlueter, A. Dieter
European Journal of Organic Chemistry, 2001 , # 20 p. 3819 - 3829
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene
Suzuki cross-coupling; Heating;
参考文献
Beinhoff, Matthias; Weigel, Wilfried; Jurczok, Martin; Rettig, Wolfgang; Modrakowski, Claudia; Bruedgam, Irene; Hartl, Hans; Schlueter, A. Dieter
European Journal of Organic Chemistry, 2001 , # 20 p. 3819 - 3829
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene
Suzuki cross-coupling; Heating;
参考文献
Beinhoff, Matthias; Weigel, Wilfried; Jurczok, Martin; Rettig, Wolfgang; Modrakowski, Claudia; Bruedgam, Irene; Hartl, Hans; Schlueter, A. Dieter
European Journal of Organic Chemistry, 2001 , # 20 p. 3819 - 3829
