2,6-二氨基-3,5-二硝基吡啶合成路线 （共 9 条）
反应条件
1: With sulfur trioxide; nitric acid; sulfuric acid T=0 - 10°C; 4 h; 2: With ammonia in water Purification / work up;
参考文献
US2009/137814 A1, ;
Page/Page column 8 ;
反应条件
1: With sulfuric acid; sulfur trioxide T=0 - 20°C; 2: With nitric acid T=0 - 15°C;
参考文献
Wang, Yanhong; Hu, Zhen; Meng, Xiangli; Jing, Jiehui; Song, Yuanjun; Zhang, Chunhua; Huang, Yudong
Molecules, 2009 , vol. 14, # 5 p. 1652 - 1659
反应条件
potassium permanganate; ammonia 1 h;
参考文献
Journal of Organic Chemistry, , vol. 50, # 4 p. 484 - 487
反应条件
sulfuric acid; nitric acid T=60 - 65°C; 1 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 33, # 3 p. 895 - 904
反应条件
sulfuric acid; nitric acid T=15°C; 2 h;
参考文献
Ritter, H.; Licht, H. H.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 2 p. 585 - 590
反应条件
potassium permanganate; ammonia T=-33°C; 1 h; Yields of byproduct given;
参考文献
Wozniak, Marian; Baranski, Andrzej; Szpakiewicz, Barbara
Liebigs Annalen der Chemie, 1993 , # 1 p. 7 - 10
反应条件
potassium permanganate; ammonia T=-33°C; 1 h; other substituted 3,5-dinitropyridines; quantum-mechanical calculations; Mechanism;
参考文献
Liebigs Annalen der Chemie, , # 1 p. 7 - 10
反应条件
potassium permanganate; ammonia
T=-33°C; 1 h;
参考文献
Wozniak, Marian; Baranski, Andrzej; Szpakiewicz, Barbara
Liebigs Annalen der Chemie, 1993 , # 1 p. 7 - 10
反应条件
ammonia; hydrogen; platinum on carbon in water
T=65°C; P=7224.57 Torr; 1 - 2 h; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY; MAGELLAN SYSTEMS INTERNATIONAL, LLC
Patent: WO2006/105076 A2, 2006 ;
Location in patent: Page/Page column 22-23 ;
