N-(4-氨基丁基)-5-(二甲基氨基)萘-1-磺酰胺合成路线 （共 3 条）
反应条件
in dichloromethane T=20°C; 12 h;
参考文献
Ohba, Yusuke; Kanao, Yukiko; Takatsuji, Mayuko; Ito, Motoki; Yabuta, Norikazu; Nojima, Hiroshi; Kita, Yasuyuki
Tetrahedron, 2007 , vol. 63, # 18 p. 3754 - 3761
反应条件
hydrazine hydrate in ethanol T=45°C; 24 h;
参考文献
Macchia, Marco; Salvetti, Francesca; Barontini, Silvia; Calvani, Federico; Gesi, Marco; Hamdan, Mahmoud; Lucacchini, Antonio; Pellegrini, Antonio; Soldani, Paola; Martini, Claudia
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 22 p. 3223 - 3228
反应条件
1: 1.) lithium bis(trimethylsilyl)amide / 1.) THF, 0 deg C, 30 min, 2.) THF, a) RT, 18 h, b) reflux, 10 h 2: hydrazine monohydrate / ethanol / 24 h / 45 °C View Scheme
参考文献
Macchia, Marco; Salvetti, Francesca; Barontini, Silvia; Calvani, Federico; Gesi, Marco; Hamdan, Mahmoud; Lucacchini, Antonio; Pellegrini, Antonio; Soldani, Paola; Martini, Claudia
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 22 p. 3223 - 3228
