(叔丁氧基羰基甲基)氯化三苯基磷合成路线 （共 11 条）
反应条件
in benzene T=20°C; 4 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 183, # 5 p. 1188 - 1208
反应条件
1: sodium hydroxide 2: benzene / addition at o deg C, and for 16 h at room temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 43 p. 4959 - 4962
反应条件
in benzene addition at 0 deg C, and for 16 h at room temperature; Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 25, # 43 p. 4959 - 4962
反应条件
1: NaOMe / methanol 2: TsN3 / CH2Cl2 View Scheme
参考文献
Schoellkopf,U.; Markusch,P.
Justus Liebigs Annalen der Chemie, 1971 , vol. 753, p. 143 - 150
反应条件
in N,N-dimethyl-formamide Heating;
参考文献
Nesmeyanov,N.A. et al.
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, # 3 p. 385 - 389,377 - 381
反应条件
1: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C 2: 1.) bis(trimethylsilyl)acetamide (BSA) / 1.) benzene, 0 deg C, 5 min, 2.) benzene, RT, 1 h 3: 69 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C 2: 78 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C 3: 63 percent / Oxone / tetrahydrofuran; H2O / 2 h / 25 °C View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C
2: 96 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C
3: 91 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature
View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
molecular sieve; potassium tert-butylate
1.) THF, r.t., 1 h, 2.) 15 h; Yield given. Multistep reaction;
参考文献
Kroutil, Wolfgang; Lasterra-Sanchez, M. Elena; Maddrell, Samuel J.; Mayon, Patrick; Morgan, Phillip; Roberts, Stanley M.; Thornton, Steven R.; Todd, Christine J.; Tueter, Melek
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 23 p. 2837 - 2844
反应条件
molecular sieve; potassium tert-butylate
1.) THF, r.t., 1 h, 2.) 15 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Kroutil, Wolfgang; Lasterra-Sanchez, M. Elena; Maddrell, Samuel J.; Mayon, Patrick; Morgan, Phillip; Roberts, Stanley M.; Thornton, Steven R.; Todd, Christine J.; Tueter, Melek
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 23 p. 2837 - 2844
